% recovery at 10LOR (10 ng/g) ± SD | ||||
---|---|---|---|---|
Compound name | GCB+PSA | C18+PSA | PSA | No clean-up |
Acephate | 72.8 ± 0.8(b) | 85.1 ± 0.6(a) | 76.1 ± 0.8(ab) | 52.5 ± 0.7(c) |
Acetamiprid | 98.1 ± 0.6(a) | 99.8 ± 0.03(a) | 99.6 ± 0.3(a) | 74.8 ± 0.0(b) |
Aldicarb fragment | 104.5 ± 0.4(a) | 100.5 ± 0.3(b) | 97.9 ± 0.2(b) | 70.6 ± 0.1(c) |
Amidosulfuron | 87.0 ± 0.8(b) | 74.3 ± 0.4(c) | 89.5 ± 0.1(b) | 94.3 ± 0.2(a) |
Azoxystrobin | 77.0 ± 0.7(b) | 108.8 ± 0.8(a) | 106.5 ± 0.8(a) | 101.8 ± 0.5(a) |
Benalaxyl | 88.9 ± 0.6(a) | 97.3 ± 1.0(a) | 97.5 ± 0.4(a) | 97.7 ± 0.6(a) |
Bifenazate | 23.7 ± 0.8(b) | 117.5 ± 0.3(a) | 111.6 ± 1.2(a) | 121.6 ± 0.4(a) |
Bifenthrin | 45.7 ± 1.1(b) | 92.5 ± 0.9(a) | 79.8 ± 0.8(a) | 90.2 ± 0.02(a) |
Bitertanol | 88.9 ± 0.6(b) | 105.6 ± 0.4(a) | 99.4 ± 0.01(a) | 100.6 ± 0.7(a,b) |
Bosclid (Nicobifen) | 39.6 ± 1.0(b) | 113.1 ± 1.3(a) | 106.3 ± 0.4(a) | 115.3 ± 0.7(a) |
Bromuconazole | 85.2 ± 1.6(b) | 96.9 ± 0.1(ab) | 103.0 ± 0.4(a) | 92.3 ± 0.4(ab) |
Bupirimate | 61.3 ± 0.6(b) | 104.6 ± 0.1(a) | 102.5 ± 0.6(a) | 110.7 ± 1.4(a) |
Buprofezin | 84.6 ± 0.5(c) | 104.0 ± 0.4(ab) | 106.9 ± 0.4(a) | 102.9 ± 0.8(b) |
Carbaryl | 98.2 ± 1.2(a) | 110.9 ± 0.9(a) | 102.5 ± 0.2(a) | 72.6 ± 0.1(b) |
Carbofuran | 108.3 ± 0.8(b) | 120.4 ± 0.9(a) | 119.9 ± 0.1(ab) | 64.1 ± 0.6(c) |
Chlorfenvinphos | 78.1 ± 0.7(c) | 93.6 ± 0.1(b) | 103.6 ± 0.2(a) | 94.9 ± 0.7(b) |
Chlorpyrifos | 21.4 ± 0.6(b) | 93.4 ± 0.6(a) | 94.2 ± 0.3(a) | 87.6 ± 1.0(a) |
Chlorpyrifos-methyl | 26.4 ± 0.8(c) | 105.3 ± 0.5(a) | 99.5 ± 0.1(a) | 95.5 ± 0.4(b) |
Clofentezin | 6.2 ± 0.7(b) | 97.3 ± 0.3(a) | 98.5 ± 0.3(a) | 91.1 ± 0.8(a) |
Coumaphos | 5.4 ± 0.4(b) | 102.6 ± 1.3(a) | 105.2 ± 0.5(a) | 109.2 ± 0.5(a) |
Cyazofamid | 79.1 ± 0.2(c) | 102.2 ± 0.1(a) | 100.6 ± 0.2(a) | 92.3 ± 0.2(b) |
Cymiazol | 56.0 ± 0.9(c) | 92.2 ± 0.4(a) | 89.5 ± 0.1(a) | 75.2 ± 0.5(a) |
Cyproconazole | 100.3 ± 0.2(b) | 87.8 ± 1.0(b) | 106.8 ± 0.2(a) | 92.3 ± 0.5(b) |
Cyprodinil | 10.5 ± 0.6(c) | 90.8 ± 0.2(b) | 104.5 ± 0.4(a) | 105.0 ± 1.0(ab) |
DEET | 109.1 ± 0.4(a) | 100.4 ± 1.2(a) | 96.0 ± 0.0(a) | 83.5 ± 0.5(b) |
Diazinon | 81.4 ± 0.01(b) | 98.7 ± 0.3(a) | 99.0 ± 0.3(a) | 99.4 ± 1.1(a) |
Dichlorvos | 107.0 ± 0.8(a) | 97.3 ± 0.6(b) | 99.4 ± 0.3(b) | 85.7 ± 0.2(c) |
Diflubenzuron | 18.9 ± 4.8(b) | 101.9 ± 0.3(a) | 106.3 ± 1(a) | 104.8 ± 0.6(a) |
Dimethoate | 99.2 ± 1.0(a) | 101.7 ± 0.2(a) | 94.3 ± 0.3(a) | 62.8 ± 0.1(b) |
Diuron | 33.0 ± 0.8(c) | 100.7 ± 0.6(a) | 108.1 ± 0.2(a) | 92.1 ± 0.4(b) |
Epoxyconazol | 38.8 ± 2.6(b) | 91.2 ± 0.2(a) | 96.4 ± 1.1(a) | 89.9 ± 0.6(a) |
Ethion | 78.7 ± 0.2(b) | 98.3 ± 0.1(a) | 103.0 ± 0.5(a) | 95.1 ± 0.1(a) |
Ethoprophos | 87.7 ± 0.9(a) | 94.1 ± 0.4(a) | 98.3 ± 1.0(a) | 90.8 ± 0.7(a) |
Etofenprox | 24.2 ± 0.5(b) | 98.5 ± 0.4(a) | 99.5 ± 0.1(a) | 92.2 ± 0.0(a) |
Fenamiphos | 56.4 ± 1.0(b) | 107.8 ± 0.2(a) | 111.6 ± 0.3(a) | 107.8 ± 0.5(a) |
Fenazaquin | 9.9 ± 1.7(d) | 93.5 ± 0.5(b) | 98.4 ± 0.1(a) | 89.4 ± 0.1(c) |
Fenbuconazole | 40.5 ± 1.2(b) | 107.8 ± 0.3(a) | 109.1 ± 0.9(a) | 107.0 ± 0.3(a) |
Fenobucarb | 94.7 ± 2.0(b) | 80.6 ± 0.4(c) | 101.6 ± 0.1(a) | 90.4 ± 0.2(b) |
Fipronil | 107.9 ± 1.0(a) | 111.4 ± 0.1(a) | 108.3 ± 0.3(a) | 111.1 ± 0.4(a) |
Flazasulfuron | 81.1 ± 1.5(b) | 46.7 ± 0.5(d) | 70.3 ± 0.3(c) | 96.7 ± 0.4(a) |
Fludioxonil | 34.1 ± 2.9(b | 105.9 ± 0.5(a) | 104.7 ± 0.1(a) | 110.8 ± 0.5(a) |
Flufenacet | 102.8 ± 1.9(a) | 117.5 ± 0.9(a) | 103.8 ± 0.7(a) | 100.9 ± 0.5(a) |
Fluquinconazole | 43.6 ± 2.0(b) | 92.7 ± 1.1(a) | 99.3 ± 0.9(a) | 90.5 ± 0.9(a) |
Flusilazole | 97.8 ± 0.8(b) | 117.4 ± 0.7(a) | 108.3 ± 0.8(ab) | 98.6 ± 0.5(ab) |
Flutriafol | 94.3 ± 0.2(b) | 97.9 ± 0.4(ab) | 101.3 ± 0.1(a) | 96.8 ± 0.5(ab) |
Fosthiazate | 101.8 ± 0.2(a) | 107.1 ± 0.9(a) | 103.6 ± 0.1(a) | 70.1 ± 0.1(b) |
Hexaconazole | 90.0 ± 1.0(b) | 99.3 ± 1.1(b) | 110.5 ± 0.5(a) | 97.9 ± 0.1(b) |
Hexythiazox | 77.2 ± 0.6(c) | 99.8 ± 0.1(a) | 99.6 ± 0.2(a) | 94.1 ± 0.4(b) |
Imidacloprid | 80.3 ± 0.2(a) | 88.3 ± 0.2(a) | 87.6 ± 0.3(a) | 66.4 ± 0.3(b) |
Indoxacarb | 56.4 ± 1.6(b) | 103.0 ± 0.5(a) | 102.1 ± 0.1(a) | 96.1 ± 0.3(a) |
Ipconazole | 57.7 ± 0.9(b) | 103.7 ± 0.2(a) | 102.7 ± 0.1(a) | 98.9 ± 0.5(a) |
Iprovalicarb | 58.6 ± 6.5(a) | 95.6 ± 0.1(a) | 99.1 ± 1.3(a) | 74.5 ± 1.2(a) |
Isoxaflutole | 99.0 ± 0.3(a) | 98.9 ± 0.5(a) | 105.6 ± 0.4(a) | 120.8 ± 2.0(a) |
Kresoxim-methyl | 74.7 ± 0.2(a) | 96.0 ± 1.1(a) | 93.1 ± 0.3(a) | 92.3 ± 0.8(a) |
Linuron | 39.7 ± 3.4(b) | 103.3 ± 0.03(a) | 107.9 ± 0.5(a) | 97.5 ± 0.1(a) |
Lufenuron | 5.9 ± 3.2(d) | 105.1 ± 0.4(a) | 98.6 ± 0.2(b) | 95.4 ± 0.2(c) |
Malathion | 102.9 ± 0.2(a) | 113.6 ± 0.2(a) | 109.4 ± 0.3(a) | 98.1 ± 0.1(a) |
Metalaxyl | 100.3 ± 0.1(a) | 102.8 ± 0.4(a) | 108.1 ± 0.2(a) | 99.3 ± 0.5(a) |
Metconazole | 56.8 ± 1.7(b) | 101.8 ± 0.8(a) | 109.9 ± 0.1(a) | 101.2 ± 0.2(a) |
Methidathion | 76.4 ± 0.7(b) | 98.2 ± 0.4(a) | 99.8 ± 0.5(a) | 77.7 ± 0.2(b) |
Methomyl | 63.9 ± 7.9(a) | 111.1 ± 0.6(a) | 105.6 ± 0.3(a) | 86.0 ± 0.4(a) |
Metolachlor | 88.6 ± 0.3(a) | 100.2 ± 0.1(a) | 97.7 ± 0.3(a) | 98.4 ± 0.9(a) |
Metribuzin | 106.3 ± 0.1(a) | 103.9 ± 0.5(a) | 106.0 ± 0.5(a) | 48.7 ± 0.3(b) |
Metsulfuron-methyl | 72.7 ± 1.7(b) | 46.6 ± 0.7(c) | 72.8 ± 0.5(b) | 122.1 ± 0.4(a) |
Monocrotophos | 86.4 ± 0.1(a) | 98.4 ± 0.2(a) | 86.3 ± 0.3(a) | 14.7 ± 7.1(b) |
Nicosulfuron | 43.9 ± 2.5(b) | 19.0 ± 1.4(c) | 42.6 ± 0.3(b) | 100.6 ± 2.1(a) |
Novaluron | 16.5 ± 2.5(c) | 104.4 ± 0.2(a) | 107.4 ± 0.3(a) | 92.1 ± 0.6(b) |
Omethoat | 88.0 ± 0.2(b) | 90.6 ± 0.2(a) | 86.4 ± 0.3(b) | 83.5 ± 0.1(b) |
Oxamyl | 90.3 ± 0.1(a) | 94.7 ± 0.0(a) | 94.4 ± 0.1(a) | 67.8 ± 0.2(b) |
Picoxystrobin | 76.7 ± 0.1(b) | 94.3 ± 0.5(a) | 92.6 ± 1.1(a) | 79.1 ± 0.3(b) |
Pirimicarb | 37.1 ± 2.2(c) | 103.6 ± 1.1(a) | 102.3 ± 0.5(a) | 81.2 ± 0.5(b) |
Pirimiphos-methyl | 44.6 ± 1.1(b) | 99.2 ± 1.1(a) | 99.1 ± 0.2(a) | 91.2 ± 0.2(a) |
Prochloraz | 34.1 ± 3.7(b) | 106.5 ± 0.4(a) | 111.4 ± 0.4(a) | 103.6 ± 0.1(a) |
Procymidon | 54.1 ± 1.0(a) | 78.8 ± 0.7(a) | 58.3 ± 1.7(a) | 66.5 ± 0.7(a) |
Profenofos | 31.7 ± 2.6(b) | 95.9 ± 0.7(a) | 97.2 ± 0.2(a) | 89.1 ± 0.4(a) |
Promecarb | 106.6 ± 0.4(a) | 107.8 ± 0.1(a) | 102.6 ± 0.2(a) | 95.1 ± 0.1(a) |
Propamocarb | 75.9 ± 0.0(a) | 49.3 ± 0.7(c) | 57.9 ± 0.2(b) | 73.4 ± 0.1(a) |
Propargit | 70.1 ± 1.4(ab) | 98.7 ± 0.4(a) | 99.4 ± 0.7(a) | 64.2 ± 0.2(ab) |
Pyraclostrobin | 5.2 ± 0.9(c) | 111.8 ± 0.0(a) | 106.7 ± 0.2(a) | 100.3 ± 0.3(b) |
Pyridaben | 53.1 ± 2.0(b) | 100.0 ± 0.8(a) | 102.6 ± 0.3(a) | 89.9 ± 1.3(a) |
Pyriproxyfen | 36.9 ± 2.6(b) | 98.1 ± 0.5(a) | 97.9 ± 0.3(a) | 92.3 ± 0.1(a) |
Rotenone | 46.7 ± 2.7(b) | 101.2 ± 0.5(a) | 100.1 ± 0.5(a) | 96.5 ± 0.1(a) |
Spinosyn A | 12.5 ± 2.6(d) | 98.3 ± 0.3(b) | 109.2 ± 0.7(a) | 87.0 ± 0.5(c) |
Spinosyn D | 9.3 ± 3.2(c) | 92.0 ± 0.1(b) | 101.6 ± 0.4(a) | 90.5 ± 0.3(b) |
Tebuconazole | 59.7 ± 1.6(b) | 99.5 ± 0.7(a) | 114.4 ± 0.6(a) | 111.4 ± 0.4(a) |
Tebufenozid | 100.9 ± 0.5(b) | 112.0 ± 0.4(a) | 120.4 ± 1.5(a) | 98.6 ± 0.4(b) |
Temephos | 25.4 ± 3.0(c) | 105.9 ± 0.4(a) | 100.7 ± 0.2(ab) | 98.0 ± 0.6(b) |
Tetraconazole | 92.5 ± 0.6(c) | 108.2 ± 1.0(a) | 102.4 ± 0.5(ab) | 93.4 ± 0.6(bc) |
Thiabendazol | 17.2 ± 1.6(d) | 82.2 ± 0.4(a) | 77.3 ± 0.1(b) | 57.9 ± 0.2(c) |
Thiacloprid | 85.3 ± 1.2(a) | 99.5 ± 0.6(a) | 94.7 ± 0.0(a) | 61.0 ± 0.3(b) |
Thiamethoxam | 95.6 ± 0.6(a) | 101.2 ± 0.1(a) | 99.7 ± 0.2(a) | 59.7 ± 0.1(b) |
Thiodicarb | 43.3 ± 2.4(c) | 101.4 ± 0.6(a) | 103.5 ± 0.5(a) | 76.8 ± 0.3(b) |
Triadimenol | 92.8 ± 0.1(b) | 108.6 ± 1.0(a) | 111.3 ± 0.03(a) | 97.9 ± 0.6(a) |
Triadimefon | 117.7 ± 0.3(a) | 107.4 ± 0.8(a) | 115.7 ± 0.1(a) | 110.6 ± 0.7(a) |
Tribenuron-methyl | 64.2 ± 1.7(b) | 73.3 ± 0.1(a) | 81.5 ± 0.1(a) | 63.4 ± 0.4(b) |
Trifloxystrobin | 60.1 ± 1.7(b) | 101.2 ± 0.2(a) | 103.8 ± 0.1(a) | 93.7 ± 0.1(a) |